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a) Synthse n 1 :a) Synthesis n 1: Dans chacune des 8 fioles de 20 mL sont ajouts 5 mL de solution de chlorure de fer III (2,7 mg/ml) et 5 mL de solution d'acide fumarique (1,16 mg/ml) : - 4 fioles servent de tmoin o les ractions sont ralises pour les 4 temps de synthse : 30, 60, 90 et 120 min,In each of the 8 vials of 20 ml are added 5 ml of iron III chloride solution (2.7 mg / ml) and 5 ml of fumaric acid solution (1.16 mg / ml): control where the reactions are carried out for the 4 synthesis times: 30, 60, 90 and 120 min, - dans les 4 autres fioles, 5 mg de PEG sont ajouts 15 min avant la fin de chacune des synthses de dure 30, 60, 90 et 120 min (la fin d'une synthse correspond la sortie du bain ultrasons ) .in the other 4 flasks, 5 mg of PEG are added 15 min before the end of each of the syntheses of duration 30, 60, 90 and 120 min (the end of a synthesis corresponds to the exit of the ultrasonic bath)

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The IRRC's objectives were described as, "The reduction, elimination, or neutralization of systems which directly or indirectly support the illegal trafficking and sales of cigarettes within the jurisdictional boundaries of our membership states."[70] The group was a "service organization" with no law enforcement powers.[71] It collected information and facilitated the exchange of information among the member states, made recommendations to states and "conduct[ed] 'tactical' operations in source states, using informants, sophisticated equipment and vehicles, and surveil[led] smugglers into the home states of the group." [72] The IRRC also pushed for federal involvement in fighting cigarette crime, including federal legislation and federal prosecution of "wholesalers who conspired with smugglers."[73] The group took credit for returning $300,000 to its members through the sale of contraband and collected cigarette taxes in its first few months